Matrix Spiking Solution, 1.2ml, nonane

2,2',4,4',6-Pentabromo-6'-hydroxy[13C12]diphenyl ether, 1.2ml x 50ug/ml, toluene

Sulfur Calibration Mixtures: Di-n-butyl sulfide in Heavy White Oil (less than 20mg/kg S) Unit : 10mL screw-capped bottle Light White Mineral Oil Heavy White Mineral Oil (20 cSt at 40°C) (70 cSt at 40°C)

Appendix IX Semi-Volatiles Mix #13