Method 4 Standard 1

2-Perfluorooctyl-[1,1-2H2]-[1,2-13C2]-ethanol (8:2), 50µg/ml in MeOH, 1,2ml

Sulfur Calibration Mixtures: Di-n-butyl sulfide in Light White Oil (less than 20mg/kg S) Unit : 10mL screw-capped bottle Light White Mineral Oil Heavy White Mineral Oil (20 cSt at 40°C) (70 cSt at 40°C)

Mandipropamid, 100 µg/ml, Acetonitrile, 5ml